Rapid-synthesis of zeolite T via sonochemical-assisted hydrothermal growth method

Sonochemical-assisted method has been identified as one of the potential pre-treatment methods which could reduce the formation duration of zeolite as well as other microporous and mesoporous materials. In the present work, zeolite T was synthesized via sonochemical-assisted pre-treatment prior to h...

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Main Authors: Jusoh, N., Yeong, Y.F., Mohamad, M., Lau, K.K., Shariff, A.M.
Format: Article
Institution: Universiti Teknologi Petronas
Record Id / ISBN-0: utp-eprints.19729 /
Published: Elsevier B.V. 2017
Online Access: https://www.scopus.com/inward/record.uri?eid=2-s2.0-84971529394&doi=10.1016%2fj.ultsonch.2016.05.033&partnerID=40&md5=aa9a5d71a7f6cfb6ea9fed438d2ab02a
http://eprints.utp.edu.my/19729/
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spelling utp-eprints.197292018-04-20T07:34:36Z Rapid-synthesis of zeolite T via sonochemical-assisted hydrothermal growth method Jusoh, N. Yeong, Y.F. Mohamad, M. Lau, K.K. Shariff, A.M. Sonochemical-assisted method has been identified as one of the potential pre-treatment methods which could reduce the formation duration of zeolite as well as other microporous and mesoporous materials. In the present work, zeolite T was synthesized via sonochemical-assisted pre-treatment prior to hydrothermal growth. The durations for sonochemical-assisted pre-treatment were varied from 30 min to 90 min. Meanwhile, the hydrothermal growth durations were ranged from 0.5 to 3 days. The physicochemical properties of the resulting samples were characterized using XRD, FESEM, FTIR and BET. As verified by XRD, the samples synthesized via hydrothermal growth durations of 1, 2 and 3 days and sonochemical-assisted pre-treatment durations of 60 min and 90 min demonstrated zeolite T structure. The samples which underwent sonochemical-assisted pre-treatment duration of 60 min yielded higher crystallinity with negligible change of zeolite T morphology. Overall, the lengthy synthesis duration of zeolite T has been successfully reduced from 7 days to 1 day by applying sonochemical-assisted pre-treatment of 60 min, while synthesis duration of 0.5 days via sonochemical-assisted pre-treatment of 60 min was not sufficient to produce zeolite T structure. © 2016 Published by Elsevier B.V. Elsevier B.V. 2017 Article PeerReviewed https://www.scopus.com/inward/record.uri?eid=2-s2.0-84971529394&doi=10.1016%2fj.ultsonch.2016.05.033&partnerID=40&md5=aa9a5d71a7f6cfb6ea9fed438d2ab02a Jusoh, N. and Yeong, Y.F. and Mohamad, M. and Lau, K.K. and Shariff, A.M. (2017) Rapid-synthesis of zeolite T via sonochemical-assisted hydrothermal growth method. Ultrasonics Sonochemistry, 34 . pp. 273-280. http://eprints.utp.edu.my/19729/
institution Universiti Teknologi Petronas
collection UTP Institutional Repository
description Sonochemical-assisted method has been identified as one of the potential pre-treatment methods which could reduce the formation duration of zeolite as well as other microporous and mesoporous materials. In the present work, zeolite T was synthesized via sonochemical-assisted pre-treatment prior to hydrothermal growth. The durations for sonochemical-assisted pre-treatment were varied from 30 min to 90 min. Meanwhile, the hydrothermal growth durations were ranged from 0.5 to 3 days. The physicochemical properties of the resulting samples were characterized using XRD, FESEM, FTIR and BET. As verified by XRD, the samples synthesized via hydrothermal growth durations of 1, 2 and 3 days and sonochemical-assisted pre-treatment durations of 60 min and 90 min demonstrated zeolite T structure. The samples which underwent sonochemical-assisted pre-treatment duration of 60 min yielded higher crystallinity with negligible change of zeolite T morphology. Overall, the lengthy synthesis duration of zeolite T has been successfully reduced from 7 days to 1 day by applying sonochemical-assisted pre-treatment of 60 min, while synthesis duration of 0.5 days via sonochemical-assisted pre-treatment of 60 min was not sufficient to produce zeolite T structure. © 2016 Published by Elsevier B.V.
format Article
author Jusoh, N.
Yeong, Y.F.
Mohamad, M.
Lau, K.K.
Shariff, A.M.
spellingShingle Jusoh, N.
Yeong, Y.F.
Mohamad, M.
Lau, K.K.
Shariff, A.M.
Rapid-synthesis of zeolite T via sonochemical-assisted hydrothermal growth method
author_sort Jusoh, N.
title Rapid-synthesis of zeolite T via sonochemical-assisted hydrothermal growth method
title_short Rapid-synthesis of zeolite T via sonochemical-assisted hydrothermal growth method
title_full Rapid-synthesis of zeolite T via sonochemical-assisted hydrothermal growth method
title_fullStr Rapid-synthesis of zeolite T via sonochemical-assisted hydrothermal growth method
title_full_unstemmed Rapid-synthesis of zeolite T via sonochemical-assisted hydrothermal growth method
title_sort rapid-synthesis of zeolite t via sonochemical-assisted hydrothermal growth method
publisher Elsevier B.V.
publishDate 2017
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-84971529394&doi=10.1016%2fj.ultsonch.2016.05.033&partnerID=40&md5=aa9a5d71a7f6cfb6ea9fed438d2ab02a
http://eprints.utp.edu.my/19729/
_version_ 1741196253596745728
score 11.62408

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