Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs

Vertically aligned Boron nitride nanotubes (BNNTs) have exceptional electrical, mechanical and thermal properties suitable for its potential applications without any further purification. However, the synthesis of aligned BNNTs via previously reported techniques is not only complicated, lengthy and...

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Main Authors: Ahmad, P., Khandaker, M.U., Muhammad, N., Rehman, F., Khan, G., Khan, A.S., Ullah, Z., Rehman, M.A., Ahmed, S., Gulzar, M., Din, I.U., Ahmed, S.M., Ali, H., Arshid, N.
Format: Article
Institution: Universiti Teknologi Petronas
Record Id / ISBN-0: utp-eprints.21827 /
Published: Elsevier Ltd 2018
Online Access: https://www.scopus.com/inward/record.uri?eid=2-s2.0-85032013805&doi=10.1016%2fj.materresbull.2017.10.031&partnerID=40&md5=0866cef40a1711d745f253f4b9ea346d
http://eprints.utp.edu.my/21827/
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spelling utp-eprints.218272018-08-01T02:02:14Z Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs Ahmad, P. Khandaker, M.U. Muhammad, N. Rehman, F. Khan, G. Khan, A.S. Ullah, Z. Rehman, M.A. Ahmed, S. Gulzar, M. Din, I.U. Ahmed, S.M. Ali, H. Arshid, N. Vertically aligned Boron nitride nanotubes (BNNTs) have exceptional electrical, mechanical and thermal properties suitable for its potential applications without any further purification. However, the synthesis of aligned BNNTs via previously reported techniques is not only complicated, lengthy and misleading but also result in useless impurities in the final product. Here, we report Magnesium diboride (MgB2) as an effective and novel precursor for the synthesis of vertically aligned BNNTs directly on SiO2 substrate at 1000 °C. Magnesium (Mg) from MgB2 in partially melted form diffuses on SiO2 substrate whereas the adsorbed Boron with Mg reacts with Nitrogen from decomposed ammonia and synthesized vertically aligned BNNTs. The morphology, alignment, structure and compositions of the as-synthesized BNNTs are studied via field emission scanning electron microscope, high resolution transmission electron microscope, energy dispersive x-ray spectroscopy, x-ray diffraction, Raman spectroscopy and Fourier transform infrared spectroscopy. © 2017 Elsevier Ltd Elsevier Ltd 2018 Article NonPeerReviewed https://www.scopus.com/inward/record.uri?eid=2-s2.0-85032013805&doi=10.1016%2fj.materresbull.2017.10.031&partnerID=40&md5=0866cef40a1711d745f253f4b9ea346d Ahmad, P. and Khandaker, M.U. and Muhammad, N. and Rehman, F. and Khan, G. and Khan, A.S. and Ullah, Z. and Rehman, M.A. and Ahmed, S. and Gulzar, M. and Din, I.U. and Ahmed, S.M. and Ali, H. and Arshid, N. (2018) Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs. Materials Research Bulletin, 98 . pp. 235-239. http://eprints.utp.edu.my/21827/
institution Universiti Teknologi Petronas
collection UTP Institutional Repository
description Vertically aligned Boron nitride nanotubes (BNNTs) have exceptional electrical, mechanical and thermal properties suitable for its potential applications without any further purification. However, the synthesis of aligned BNNTs via previously reported techniques is not only complicated, lengthy and misleading but also result in useless impurities in the final product. Here, we report Magnesium diboride (MgB2) as an effective and novel precursor for the synthesis of vertically aligned BNNTs directly on SiO2 substrate at 1000 °C. Magnesium (Mg) from MgB2 in partially melted form diffuses on SiO2 substrate whereas the adsorbed Boron with Mg reacts with Nitrogen from decomposed ammonia and synthesized vertically aligned BNNTs. The morphology, alignment, structure and compositions of the as-synthesized BNNTs are studied via field emission scanning electron microscope, high resolution transmission electron microscope, energy dispersive x-ray spectroscopy, x-ray diffraction, Raman spectroscopy and Fourier transform infrared spectroscopy. © 2017 Elsevier Ltd
format Article
author Ahmad, P.
Khandaker, M.U.
Muhammad, N.
Rehman, F.
Khan, G.
Khan, A.S.
Ullah, Z.
Rehman, M.A.
Ahmed, S.
Gulzar, M.
Din, I.U.
Ahmed, S.M.
Ali, H.
Arshid, N.
spellingShingle Ahmad, P.
Khandaker, M.U.
Muhammad, N.
Rehman, F.
Khan, G.
Khan, A.S.
Ullah, Z.
Rehman, M.A.
Ahmed, S.
Gulzar, M.
Din, I.U.
Ahmed, S.M.
Ali, H.
Arshid, N.
Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
author_sort Ahmad, P.
title Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
title_short Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
title_full Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
title_fullStr Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
title_full_unstemmed Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
title_sort magnesium diboride (mgb2): an effective and novel precursor for the synthesis of vertically aligned bnnts
publisher Elsevier Ltd
publishDate 2018
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-85032013805&doi=10.1016%2fj.materresbull.2017.10.031&partnerID=40&md5=0866cef40a1711d745f253f4b9ea346d
http://eprints.utp.edu.my/21827/
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