Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes

In the past few years, composite membrane has been introduced to cater the limitation of polymeric and inorganic membranes. However, the fabrication of ideal composite membrane with appropriate loading of filler remains challenging. Thus, the material selection as well as optimum loading with the co...

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Main Authors: Kamarudin, M.S., Jusoh, N., Tengku Hassan, T.N.A., Md Ali, U.F., Abdullah, S.B., Amir Hamzah, A.S.S.S.
Format: Conference or Workshop Item
Institution: Universiti Teknologi Petronas
Record Id / ISBN-0: utp-eprints.29683 /
Published: Elsevier Ltd 2020
Online Access: https://www.scopus.com/inward/record.uri?eid=2-s2.0-85116443568&doi=10.1016%2fj.matpr.2021.02.793&partnerID=40&md5=8b52a2d2e91eada115b54d76793a5189
http://eprints.utp.edu.my/29683/
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spelling utp-eprints.296832022-03-25T02:35:55Z Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes Kamarudin, M.S. Jusoh, N. Tengku Hassan, T.N.A. Md Ali, U.F. Abdullah, S.B. Amir Hamzah, A.S.S.S. In the past few years, composite membrane has been introduced to cater the limitation of polymeric and inorganic membranes. However, the fabrication of ideal composite membrane with appropriate loading of filler remains challenging. Thus, the material selection as well as optimum loading with the conditions observed for the formulation of the composite membrane studied. In this present work, a series of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membrane with different loading of SAPO-34 particles (0-4 wt) were fabricated. The physicochemical properties of the resultant membranes were investigated by utilizing X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive X-ray (EDX). Based on analysis, a good distribution of filler was obtained for the membranes loaded with 1 wt and 2 wt of SAPO-34 particles. Further increase of inorganic filler loading lead to the sedimentation and agglomeration of particle in the membrane, which may deteriorate the membrane performance in gas separation. Therefore, the optimum loading of inorganic particles in polymer phase play a major role in obtaining membrane with minimum defects ahead of gas separation performance tests such as for CO2/ethylene separation application. © 2020 Elsevier Ltd. All rights reserved. Elsevier Ltd 2020 Conference or Workshop Item NonPeerReviewed https://www.scopus.com/inward/record.uri?eid=2-s2.0-85116443568&doi=10.1016%2fj.matpr.2021.02.793&partnerID=40&md5=8b52a2d2e91eada115b54d76793a5189 Kamarudin, M.S. and Jusoh, N. and Tengku Hassan, T.N.A. and Md Ali, U.F. and Abdullah, S.B. and Amir Hamzah, A.S.S.S. (2020) Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes. In: UNSPECIFIED. http://eprints.utp.edu.my/29683/
institution Universiti Teknologi Petronas
collection UTP Institutional Repository
description In the past few years, composite membrane has been introduced to cater the limitation of polymeric and inorganic membranes. However, the fabrication of ideal composite membrane with appropriate loading of filler remains challenging. Thus, the material selection as well as optimum loading with the conditions observed for the formulation of the composite membrane studied. In this present work, a series of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membrane with different loading of SAPO-34 particles (0-4 wt) were fabricated. The physicochemical properties of the resultant membranes were investigated by utilizing X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive X-ray (EDX). Based on analysis, a good distribution of filler was obtained for the membranes loaded with 1 wt and 2 wt of SAPO-34 particles. Further increase of inorganic filler loading lead to the sedimentation and agglomeration of particle in the membrane, which may deteriorate the membrane performance in gas separation. Therefore, the optimum loading of inorganic particles in polymer phase play a major role in obtaining membrane with minimum defects ahead of gas separation performance tests such as for CO2/ethylene separation application. © 2020 Elsevier Ltd. All rights reserved.
format Conference or Workshop Item
author Kamarudin, M.S.
Jusoh, N.
Tengku Hassan, T.N.A.
Md Ali, U.F.
Abdullah, S.B.
Amir Hamzah, A.S.S.S.
spellingShingle Kamarudin, M.S.
Jusoh, N.
Tengku Hassan, T.N.A.
Md Ali, U.F.
Abdullah, S.B.
Amir Hamzah, A.S.S.S.
Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes
author_sort Kamarudin, M.S.
title Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes
title_short Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes
title_full Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes
title_fullStr Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes
title_full_unstemmed Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes
title_sort fabrication and characterization of poly(ether-block-amide) (pebax-1657) and silicoaluminophosphate (sapo-34) composite membranes
publisher Elsevier Ltd
publishDate 2020
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-85116443568&doi=10.1016%2fj.matpr.2021.02.793&partnerID=40&md5=8b52a2d2e91eada115b54d76793a5189
http://eprints.utp.edu.my/29683/
_version_ 1741197283053010944
score 11.62408

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