Parametric study of glycerol and contaminants removal from biodiesel through solvent-aided crystallization

At present, biodiesel is known as an alternative fuel globally. It is also known that the purification of biodiesel before consumption is mandatory to comply with international standards. Commonly, purification using water washing generates a massive amount of wastewater with a high content of organ...

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Main Authors: Ahmad, M.A., Letchumanan, A., Samsuri, S., Mazli, W.N.A., Md Saad, J.
Format: Article
Institution: Universiti Teknologi Petronas
Record Id / ISBN-0: utp-eprints.30355 /
Published: Springer Science and Business Media Deutschland GmbH 2021
Online Access: https://www.scopus.com/inward/record.uri?eid=2-s2.0-85109373680&doi=10.1186%2fs40643-021-00409-y&partnerID=40&md5=5a1093df1ef7f9f62ae3467f8f548153
http://eprints.utp.edu.my/30355/
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spelling utp-eprints.303552022-03-25T06:44:15Z Parametric study of glycerol and contaminants removal from biodiesel through solvent-aided crystallization Ahmad, M.A. Letchumanan, A. Samsuri, S. Mazli, W.N.A. Md Saad, J. At present, biodiesel is known as an alternative fuel globally. It is also known that the purification of biodiesel before consumption is mandatory to comply with international standards. Commonly, purification using water washing generates a massive amount of wastewater with a high content of organic compounds that can harm the environment. Therefore, this study applied and tested a waterless method, i.e., the solvent-aided crystallization (SAC), to remove glycerol and other traces of impurities in the crude biodiesel. The parameters of coolant temperature, crystallization time, and stirring rate on the SAC system were investigated. It was discovered that with 14 °C coolant temperature, 300 RPM and higher cooling time result in the highest percentage of FAME up to 99.54, which indicates that contaminants' presence is limited in the purified biodiesel. The use of 1-butanol as the solvent for crystallization process remarkably enhanced the separation and improved the higher biodiesel quality. Figure not available: see fulltext. © 2021, The Author(s). Springer Science and Business Media Deutschland GmbH 2021 Article NonPeerReviewed https://www.scopus.com/inward/record.uri?eid=2-s2.0-85109373680&doi=10.1186%2fs40643-021-00409-y&partnerID=40&md5=5a1093df1ef7f9f62ae3467f8f548153 Ahmad, M.A. and Letchumanan, A. and Samsuri, S. and Mazli, W.N.A. and Md Saad, J. (2021) Parametric study of glycerol and contaminants removal from biodiesel through solvent-aided crystallization. Bioresources and Bioprocessing, 8 (1). http://eprints.utp.edu.my/30355/
institution Universiti Teknologi Petronas
collection UTP Institutional Repository
description At present, biodiesel is known as an alternative fuel globally. It is also known that the purification of biodiesel before consumption is mandatory to comply with international standards. Commonly, purification using water washing generates a massive amount of wastewater with a high content of organic compounds that can harm the environment. Therefore, this study applied and tested a waterless method, i.e., the solvent-aided crystallization (SAC), to remove glycerol and other traces of impurities in the crude biodiesel. The parameters of coolant temperature, crystallization time, and stirring rate on the SAC system were investigated. It was discovered that with 14 °C coolant temperature, 300 RPM and higher cooling time result in the highest percentage of FAME up to 99.54, which indicates that contaminants' presence is limited in the purified biodiesel. The use of 1-butanol as the solvent for crystallization process remarkably enhanced the separation and improved the higher biodiesel quality. Figure not available: see fulltext. © 2021, The Author(s).
format Article
author Ahmad, M.A.
Letchumanan, A.
Samsuri, S.
Mazli, W.N.A.
Md Saad, J.
spellingShingle Ahmad, M.A.
Letchumanan, A.
Samsuri, S.
Mazli, W.N.A.
Md Saad, J.
Parametric study of glycerol and contaminants removal from biodiesel through solvent-aided crystallization
author_sort Ahmad, M.A.
title Parametric study of glycerol and contaminants removal from biodiesel through solvent-aided crystallization
title_short Parametric study of glycerol and contaminants removal from biodiesel through solvent-aided crystallization
title_full Parametric study of glycerol and contaminants removal from biodiesel through solvent-aided crystallization
title_fullStr Parametric study of glycerol and contaminants removal from biodiesel through solvent-aided crystallization
title_full_unstemmed Parametric study of glycerol and contaminants removal from biodiesel through solvent-aided crystallization
title_sort parametric study of glycerol and contaminants removal from biodiesel through solvent-aided crystallization
publisher Springer Science and Business Media Deutschland GmbH
publishDate 2021
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-85109373680&doi=10.1186%2fs40643-021-00409-y&partnerID=40&md5=5a1093df1ef7f9f62ae3467f8f548153
http://eprints.utp.edu.my/30355/
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