Extraction of biocompatible hydroxyapatite from fish scales using novel approach of ionic liquid pretreatment

In this study the waste fish scales (FS) were dissolved in 1-butyl-3-methylimidazolium acetate ionic liquid to obtain a valuable product of hydroxyapatite (HAp). The HAp was obtained in the yield of 32 ± 2. The obtained HAp was characterized using Fourier Transform Infrared Spectroscopy (FTIR), Pow...

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Main Authors: Muhammad, N., Gao, Y., Iqbal, F., Ahmad, P., Ge, R., Nishan, U., Rahim, A., Gonfa, G., Ullah, Z.
Format: Article
Institution: Universiti Teknologi Petronas
Record Id / ISBN-0: utp-eprints.30950 /
Published: Elsevier 2016
Online Access: https://www.scopus.com/inward/record.uri?eid=2-s2.0-84956934336&doi=10.1016%2fj.seppur.2016.01.047&partnerID=40&md5=c4d0bbcf962f056f2cc466589bebd17e
http://eprints.utp.edu.my/30950/
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spelling utp-eprints.309502022-03-25T07:51:48Z Extraction of biocompatible hydroxyapatite from fish scales using novel approach of ionic liquid pretreatment Muhammad, N. Gao, Y. Iqbal, F. Ahmad, P. Ge, R. Nishan, U. Rahim, A. Gonfa, G. Ullah, Z. In this study the waste fish scales (FS) were dissolved in 1-butyl-3-methylimidazolium acetate ionic liquid to obtain a valuable product of hydroxyapatite (HAp). The HAp was obtained in the yield of 32 ± 2. The obtained HAp was characterized using Fourier Transform Infrared Spectroscopy (FTIR), Powder X-rays Diffraction (PXRD), Thermal Gravimetric Analysis (TGA), Field Emission Scanning Microscopy (FE-SEM), Energy Dispersive X-rays spectroscopy (EDX), and Brunauer-Emmett-Teller (BET). The results of FTIR and XRD showed the characteristic peaks of the HAp. The thermal degradation temperature of the extracted HAp was relatively high. Furthermore, low weight loss was measured which confirmed the removal of organic part of FS during ionic liquid treatment. The FE-SEM result showed the particles with different morphologies and EDX analysis showed a Ca/P ratio of 1.60 for the extracted HAp. The biocompatibility of the extracted HAp was assessed through MTT cell viability assay using known Human Embryonic Kidney 293 cells (HEK cells) and epidermoid carcinoma cells (A431 cells). © 2016 Elsevier B.V. All rights reserved. Elsevier 2016 Article NonPeerReviewed https://www.scopus.com/inward/record.uri?eid=2-s2.0-84956934336&doi=10.1016%2fj.seppur.2016.01.047&partnerID=40&md5=c4d0bbcf962f056f2cc466589bebd17e Muhammad, N. and Gao, Y. and Iqbal, F. and Ahmad, P. and Ge, R. and Nishan, U. and Rahim, A. and Gonfa, G. and Ullah, Z. (2016) Extraction of biocompatible hydroxyapatite from fish scales using novel approach of ionic liquid pretreatment. Separation and Purification Technology, 161 . pp. 129-135. http://eprints.utp.edu.my/30950/
institution Universiti Teknologi Petronas
collection UTP Institutional Repository
description In this study the waste fish scales (FS) were dissolved in 1-butyl-3-methylimidazolium acetate ionic liquid to obtain a valuable product of hydroxyapatite (HAp). The HAp was obtained in the yield of 32 ± 2. The obtained HAp was characterized using Fourier Transform Infrared Spectroscopy (FTIR), Powder X-rays Diffraction (PXRD), Thermal Gravimetric Analysis (TGA), Field Emission Scanning Microscopy (FE-SEM), Energy Dispersive X-rays spectroscopy (EDX), and Brunauer-Emmett-Teller (BET). The results of FTIR and XRD showed the characteristic peaks of the HAp. The thermal degradation temperature of the extracted HAp was relatively high. Furthermore, low weight loss was measured which confirmed the removal of organic part of FS during ionic liquid treatment. The FE-SEM result showed the particles with different morphologies and EDX analysis showed a Ca/P ratio of 1.60 for the extracted HAp. The biocompatibility of the extracted HAp was assessed through MTT cell viability assay using known Human Embryonic Kidney 293 cells (HEK cells) and epidermoid carcinoma cells (A431 cells). © 2016 Elsevier B.V. All rights reserved.
format Article
author Muhammad, N.
Gao, Y.
Iqbal, F.
Ahmad, P.
Ge, R.
Nishan, U.
Rahim, A.
Gonfa, G.
Ullah, Z.
spellingShingle Muhammad, N.
Gao, Y.
Iqbal, F.
Ahmad, P.
Ge, R.
Nishan, U.
Rahim, A.
Gonfa, G.
Ullah, Z.
Extraction of biocompatible hydroxyapatite from fish scales using novel approach of ionic liquid pretreatment
author_sort Muhammad, N.
title Extraction of biocompatible hydroxyapatite from fish scales using novel approach of ionic liquid pretreatment
title_short Extraction of biocompatible hydroxyapatite from fish scales using novel approach of ionic liquid pretreatment
title_full Extraction of biocompatible hydroxyapatite from fish scales using novel approach of ionic liquid pretreatment
title_fullStr Extraction of biocompatible hydroxyapatite from fish scales using novel approach of ionic liquid pretreatment
title_full_unstemmed Extraction of biocompatible hydroxyapatite from fish scales using novel approach of ionic liquid pretreatment
title_sort extraction of biocompatible hydroxyapatite from fish scales using novel approach of ionic liquid pretreatment
publisher Elsevier
publishDate 2016
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-84956934336&doi=10.1016%2fj.seppur.2016.01.047&partnerID=40&md5=c4d0bbcf962f056f2cc466589bebd17e
http://eprints.utp.edu.my/30950/
_version_ 1741197494432301056
score 11.62408

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