Effect of Photocatalysts Preparation Methods and Light Source on Orange II Photocatalytic Degradation
The objective of the present work was to synthesize 10 wt % metal doped TiO2 (Degussa P-25) photocatalysts using three methods: complex precipitation (CP), depositionprecipitation (DP) and wet impregnation (WI) methods and to evaluate their performance for a model azo dye, Orange II. The raw ph...
| Main Authors: | Riaz, Nadia, Nurlaela, Ela, Khan, M Saqib, Chong, Fai Kait, Dutta, Binay K. |
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| Format: | Article |
| Institution: | Universiti Teknologi Petronas |
| Record Id / ISBN-0: | utp-eprints.7364 / |
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IACSIT Press, Singapore
2011
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http://eprints.utp.edu.my/7364/1/25-F10114_IPCBEE_Nadia.pdf http://eprints.utp.edu.my/7364/ |
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utp-eprints.73642017-03-20T01:59:46Z Effect of Photocatalysts Preparation Methods and Light Source on Orange II Photocatalytic Degradation Riaz, Nadia Nurlaela, Ela Khan, M Saqib Chong, Fai Kait Dutta, Binay K. TP Chemical technology QD Chemistry The objective of the present work was to synthesize 10 wt % metal doped TiO2 (Degussa P-25) photocatalysts using three methods: complex precipitation (CP), depositionprecipitation (DP) and wet impregnation (WI) methods and to evaluate their performance for a model azo dye, Orange II. The raw photocatalysts were activated by calcination at three different temperatures (180°C, 200°C and 300°C) for 1 hour duration. Photocatalytic degradation for 50 ppm orange II was studied at pH 6.8 under the irradiation of a UV light and visible light. The extent of dye degradation was determined using UV-vis Spectrophotometery. On the basis of results it was observed that visible light has better effect for dye removal compared to UV light and WI photocatalysts showed the best decolorization results with 100% Orange II removal for photocatalysts calcined at 1800C and 2000C while 98.5% for 3000C calcination temperature. Selected photocatalysts were characterized using Powder X-ray Diffraction (XRD), Fieldemission Scanning Electron Microscopy-Energy Dispersive Xray (FESEM- EDX) and Diffuse Reflectance UV visible spectroscopy (DRUV vis). IACSIT Press, Singapore 2011 Article PeerReviewed application/pdf http://eprints.utp.edu.my/7364/1/25-F10114_IPCBEE_Nadia.pdf Riaz, Nadia and Nurlaela, Ela and Khan, M Saqib and Chong, Fai Kait and Dutta, Binay K. (2011) Effect of Photocatalysts Preparation Methods and Light Source on Orange II Photocatalytic Degradation. 2011 2nd International Conference on Environmental Science and Technology IPCBEE, 6 . V2-112. http://eprints.utp.edu.my/7364/ |
| institution |
Universiti Teknologi Petronas |
| collection |
UTP Institutional Repository |
| topic |
TP Chemical technology QD Chemistry |
| spellingShingle |
TP Chemical technology QD Chemistry Riaz, Nadia Nurlaela, Ela Khan, M Saqib Chong, Fai Kait Dutta, Binay K. Effect of Photocatalysts Preparation Methods and Light Source on Orange II Photocatalytic Degradation |
| description |
The objective of the present work was to synthesize
10 wt % metal doped TiO2 (Degussa P-25) photocatalysts
using three methods: complex precipitation (CP), depositionprecipitation
(DP) and wet impregnation (WI) methods and to
evaluate their performance for a model azo dye, Orange II.
The raw photocatalysts were activated by calcination at three
different temperatures (180°C, 200°C and 300°C) for 1 hour
duration. Photocatalytic degradation for 50 ppm orange II was
studied at pH 6.8 under the irradiation of a UV light and
visible light. The extent of dye degradation was determined
using UV-vis Spectrophotometery. On the basis of results it
was observed that visible light has better effect for dye removal
compared to UV light and WI photocatalysts showed the best
decolorization results with 100% Orange II removal for
photocatalysts calcined at 1800C and 2000C while 98.5% for
3000C calcination temperature. Selected photocatalysts were
characterized using Powder X-ray Diffraction (XRD), Fieldemission
Scanning Electron Microscopy-Energy Dispersive Xray
(FESEM- EDX) and Diffuse Reflectance UV visible
spectroscopy (DRUV vis). |
| format |
Article |
| author |
Riaz, Nadia Nurlaela, Ela Khan, M Saqib Chong, Fai Kait Dutta, Binay K. |
| author_sort |
Riaz, Nadia |
| title |
Effect of Photocatalysts Preparation Methods and Light Source on Orange II Photocatalytic Degradation |
| title_short |
Effect of Photocatalysts Preparation Methods and Light Source on Orange II Photocatalytic Degradation |
| title_full |
Effect of Photocatalysts Preparation Methods and Light Source on Orange II Photocatalytic Degradation |
| title_fullStr |
Effect of Photocatalysts Preparation Methods and Light Source on Orange II Photocatalytic Degradation |
| title_full_unstemmed |
Effect of Photocatalysts Preparation Methods and Light Source on Orange II Photocatalytic Degradation |
| title_sort |
effect of photocatalysts preparation methods and light source on orange ii photocatalytic degradation |
| publisher |
IACSIT Press, Singapore |
| publishDate |
2011 |
| url |
http://eprints.utp.edu.my/7364/1/25-F10114_IPCBEE_Nadia.pdf http://eprints.utp.edu.my/7364/ |
| _version_ |
1741196102683590656 |
| score |
11.62408 |