Co-precipitation synthesis of Co2+xFe2+1-xFe2O4nanoparticles: Structural characterization and magnetic properties

Cobalt ferrite is known as a promising magnetic material for various applications. This metal-ceramic composite (Cox2+Fe1-x2+Fe2O4) was synthesized via co-precipitation route, by varying the Co/Fe ratios (Co/Fe = 0.3, 0.2, and 0). The structures and magnetic properties of nano-composites were analyz...

Full description

Main Authors: Soleimani, H., Yahya, N., Latiff, N.R.A., Sabet, M., Guan, B.H., Chuan, L.K.
Format: Conference or Workshop Item
Institution: Universiti Teknologi Petronas
Record Id / ISBN-0: utp-eprints.31108 /
Published: American Institute of Physics Inc. 2014
Online Access: https://www.scopus.com/inward/record.uri?eid=2-s2.0-84969796301&doi=10.1063%2f1.4898514&partnerID=40&md5=f5a9461569870fc391942045b7af90fb
http://eprints.utp.edu.my/31108/
Tags: Add Tag
No Tags, Be the first to tag this record!
id utp-eprints.31108
recordtype eprints
spelling utp-eprints.311082022-03-25T08:59:57Z Co-precipitation synthesis of Co2+xFe2+1-xFe2O4nanoparticles: Structural characterization and magnetic properties Soleimani, H. Yahya, N. Latiff, N.R.A. Sabet, M. Guan, B.H. Chuan, L.K. Cobalt ferrite is known as a promising magnetic material for various applications. This metal-ceramic composite (Cox2+Fe1-x2+Fe2O4) was synthesized via co-precipitation route, by varying the Co/Fe ratios (Co/Fe = 0.3, 0.2, and 0). The structures and magnetic properties of nano-composites were analyzed by XRD and VSM. As deduced from the XRD line broadening, the average crystallite size of the samples was found to be in the range of 13.0-15.0 nm and contain fcc structure with smaller lattice constant as the Co/Fe ratios increases. FESEM and TEM images revealed the morphology of the samples, which consist of irregular shapes of diameter in the range of 9.0-15.0 nm. Magnetic properties measurement shows that sample S11 with the highest Co/Fe ratio has the highest value of saturation magnetization (Ms) of 65.23 emu/g. On the other hand, increase in the concentration of cobalt ions improves the remanence magnetization (Mr) and coercivity (Hc) of the same sample to 12.18 emu/g and 238.92 Oe, respectively. It is demonstrated that the higher substitution ratio of cobalt in Cox2+Fe1-x2+Fe2O4 has successfully improve the magnetic properties of the samples. © 2014 AIP Publishing LLC. American Institute of Physics Inc. 2014 Conference or Workshop Item NonPeerReviewed https://www.scopus.com/inward/record.uri?eid=2-s2.0-84969796301&doi=10.1063%2f1.4898514&partnerID=40&md5=f5a9461569870fc391942045b7af90fb Soleimani, H. and Yahya, N. and Latiff, N.R.A. and Sabet, M. and Guan, B.H. and Chuan, L.K. (2014) Co-precipitation synthesis of Co2+xFe2+1-xFe2O4nanoparticles: Structural characterization and magnetic properties. In: UNSPECIFIED. http://eprints.utp.edu.my/31108/
institution Universiti Teknologi Petronas
collection UTP Institutional Repository
description Cobalt ferrite is known as a promising magnetic material for various applications. This metal-ceramic composite (Cox2+Fe1-x2+Fe2O4) was synthesized via co-precipitation route, by varying the Co/Fe ratios (Co/Fe = 0.3, 0.2, and 0). The structures and magnetic properties of nano-composites were analyzed by XRD and VSM. As deduced from the XRD line broadening, the average crystallite size of the samples was found to be in the range of 13.0-15.0 nm and contain fcc structure with smaller lattice constant as the Co/Fe ratios increases. FESEM and TEM images revealed the morphology of the samples, which consist of irregular shapes of diameter in the range of 9.0-15.0 nm. Magnetic properties measurement shows that sample S11 with the highest Co/Fe ratio has the highest value of saturation magnetization (Ms) of 65.23 emu/g. On the other hand, increase in the concentration of cobalt ions improves the remanence magnetization (Mr) and coercivity (Hc) of the same sample to 12.18 emu/g and 238.92 Oe, respectively. It is demonstrated that the higher substitution ratio of cobalt in Cox2+Fe1-x2+Fe2O4 has successfully improve the magnetic properties of the samples. © 2014 AIP Publishing LLC.
format Conference or Workshop Item
author Soleimani, H.
Yahya, N.
Latiff, N.R.A.
Sabet, M.
Guan, B.H.
Chuan, L.K.
spellingShingle Soleimani, H.
Yahya, N.
Latiff, N.R.A.
Sabet, M.
Guan, B.H.
Chuan, L.K.
Co-precipitation synthesis of Co2+xFe2+1-xFe2O4nanoparticles: Structural characterization and magnetic properties
author_sort Soleimani, H.
title Co-precipitation synthesis of Co2+xFe2+1-xFe2O4nanoparticles: Structural characterization and magnetic properties
title_short Co-precipitation synthesis of Co2+xFe2+1-xFe2O4nanoparticles: Structural characterization and magnetic properties
title_full Co-precipitation synthesis of Co2+xFe2+1-xFe2O4nanoparticles: Structural characterization and magnetic properties
title_fullStr Co-precipitation synthesis of Co2+xFe2+1-xFe2O4nanoparticles: Structural characterization and magnetic properties
title_full_unstemmed Co-precipitation synthesis of Co2+xFe2+1-xFe2O4nanoparticles: Structural characterization and magnetic properties
title_sort co-precipitation synthesis of co2+xfe2+1-xfe2o4nanoparticles: structural characterization and magnetic properties
publisher American Institute of Physics Inc.
publishDate 2014
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-84969796301&doi=10.1063%2f1.4898514&partnerID=40&md5=f5a9461569870fc391942045b7af90fb
http://eprints.utp.edu.my/31108/
_version_ 1741197520278650880
score 11.62408