Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials

Ion-exchange of palladium (Pd) precursor for two different types of well-ordered SBA- 15 morphologies, necklace-like and rod-like, was studied. Approximately 3.8 wt Pd was successfully incorporated into SBA-15 at pH 10.3. Formation of SBA-15 and Pd/SBA-15 were characterized by Scanning Electron Micr...

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Main Authors: Lee, S.-P., Ramli, A., Kutty, M.G., Hamid, S.B.A.
Format: Article
Institution: Universiti Teknologi Petronas
Record Id / ISBN-0: utp-eprints.32345 /
Published: Trans Tech Publications Ltd 2014
Online Access: https://www.scopus.com/inward/record.uri?eid=2-s2.0-84904068481&doi=10.4028%2fwww.scientific.net%2fAMR.917.10&partnerID=40&md5=e834aa370140ff72febcbf4dd3fbe68f
http://eprints.utp.edu.my/32345/
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spelling utp-eprints.323452022-03-29T05:28:03Z Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials Lee, S.-P. Ramli, A. Kutty, M.G. Hamid, S.B.A. Ion-exchange of palladium (Pd) precursor for two different types of well-ordered SBA- 15 morphologies, necklace-like and rod-like, was studied. Approximately 3.8 wt Pd was successfully incorporated into SBA-15 at pH 10.3. Formation of SBA-15 and Pd/SBA-15 were characterized by Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), Thermogravimetry with Simultaneous Difference Thermal Spectroscopy coupled with mass spectrometer (TG/SDTA-MS), Thermogravimetry in combination with Simultaneous Difference Thermal Spectroscopy (TG-SDTA), Inductive Coupled Plasma Mass Spectrometer (ICP-MS) and N2 adsorption-desorption. Reduction of surface area and pore volume of support for Pd/SBA-15 samples may indicate the encapsulation of PdO particles within mesoporous channels of SBA-15. © (2014) Trans Tech Publications, Switzerland. Trans Tech Publications Ltd 2014 Article NonPeerReviewed https://www.scopus.com/inward/record.uri?eid=2-s2.0-84904068481&doi=10.4028%2fwww.scientific.net%2fAMR.917.10&partnerID=40&md5=e834aa370140ff72febcbf4dd3fbe68f Lee, S.-P. and Ramli, A. and Kutty, M.G. and Hamid, S.B.A. (2014) Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials. Advanced Materials Research, 917 . pp. 10-17. http://eprints.utp.edu.my/32345/
institution Universiti Teknologi Petronas
collection UTP Institutional Repository
description Ion-exchange of palladium (Pd) precursor for two different types of well-ordered SBA- 15 morphologies, necklace-like and rod-like, was studied. Approximately 3.8 wt Pd was successfully incorporated into SBA-15 at pH 10.3. Formation of SBA-15 and Pd/SBA-15 were characterized by Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), Thermogravimetry with Simultaneous Difference Thermal Spectroscopy coupled with mass spectrometer (TG/SDTA-MS), Thermogravimetry in combination with Simultaneous Difference Thermal Spectroscopy (TG-SDTA), Inductive Coupled Plasma Mass Spectrometer (ICP-MS) and N2 adsorption-desorption. Reduction of surface area and pore volume of support for Pd/SBA-15 samples may indicate the encapsulation of PdO particles within mesoporous channels of SBA-15. © (2014) Trans Tech Publications, Switzerland.
format Article
author Lee, S.-P.
Ramli, A.
Kutty, M.G.
Hamid, S.B.A.
spellingShingle Lee, S.-P.
Ramli, A.
Kutty, M.G.
Hamid, S.B.A.
Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials
author_sort Lee, S.-P.
title Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials
title_short Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials
title_full Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials
title_fullStr Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials
title_full_unstemmed Incorporation of Pd nanoparticles on rod and necklace-like SBA-15 supports materials
title_sort incorporation of pd nanoparticles on rod and necklace-like sba-15 supports materials
publisher Trans Tech Publications Ltd
publishDate 2014
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-84904068481&doi=10.4028%2fwww.scientific.net%2fAMR.917.10&partnerID=40&md5=e834aa370140ff72febcbf4dd3fbe68f
http://eprints.utp.edu.my/32345/
_version_ 1741197720745410560
score 11.62408

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